A Preparative Microwave Method for the Isomerisation of 4,16-Dibromo[2.2]Paracyclophane Into 4,12-Dibromo[2.2]Paracyclophane1

D. Christopher Braddock, Simon M. Ahmad and Gordon T. Douglas, Imperial College London

Abstract
The microwave power treatment unit is based on direct transfer of microwave energy and selective absorption of microwaves in processing materials. The characteristics of selectivity and direct transfer induce a considerable energy saving with respect to classical technologies, but it depends on the nature of the mixture.

The working parameters (total time of treatment, power level, efficiency (%) are set up on the interactive panel/display at the microcontroller unit or recalled from a PC database. This device is used as a basic tool for the research dealing with processing of condensed matter in microwave fields, especially for chemical synthesis and solid probe preparation for analysis.

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